Browsing by Author "Aksoz, Sezen"
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Article Effect of Sn contents on thermodynamic, microstructure and mechanical properties in the Zn-90-Bi-10 and Bi-88-Zn-12 based ternary alloys(SPRINGER, VAN GODEWIJCKSTRAAT 30, 3311 GZ DORDRECHT, NETHERLANDS, 2019) Esener, Pinar Ata; Altintas, Yemliha; Bayram, Umit; Ozturk, Esra; Marasli, Necmettin; Aksoz, Sezen; 0000-0002-1993-2655; 0000-0001-8760-8024; AGÜ, Mühendislik Fakültesi, Malzeme Bilimi ve Nanoteknoloji Mühendisliği BölümüThe thermal conductivity variations with temperature for Zn90-x-Sn-x-Bi10 (x=5,10, 40 and 85wt%) and Bi88-x-Sn-x-Zn-12 (x=1.39, 43.26 and 79.3wt%) alloys were measured by using the linear heat flow method. From thermal conductivity-temperature plots, the coefficients of thermal conductivity for the Zn-Sn-Bi alloys were calculated. The microstructures of Zn-Sn-Bi alloys were observed using scanning electron microscopy (SEM). The existing phases into microstructure were identified energy dispersive X-ray (EDX) analysis. The melting temperatures, the enthalpy of fusion and specific heat change between the liquid and solid phases in the Zn-Sn-Bi alloys were determined from Differential Scanning Calorimetry (DSC) trace. The tensile strength and microhardness of the alloys were measured using a Shimadzu Universal Testing Instrument (Type AG-10 KNG) and Future-Tech FM-700 model microhardness device.Article Experimental Determination of Interfacial Energies for Solid Sn in Equilibrium with Sn-Mg-Zn Liquid(KOREAN INST METALS MATERIALS, 2015) Altintas, Yemliha; Ozturk, Esra; Aksoz, Sezen; Keslioglu, Kazim; Marasli, Necmettin; AGÜ, Mühendislik Fakültesi, Malzeme Bilimi ve Nanoteknoloji Mühendisliği Bölümü; Altintas, YemlihaThe equilibrated grain boundary groove shapes of solid Sn in equilibrium with Sn-Mg-Zn liquid were observed from a quenched sample by using a radial heat flow apparatus. The Gibbs-Thomson coefficient, solid-liquid interfacial energy and grain boundary energy of solid Sn were determined from the observed grain boundary groove shapes. The thermal conductivity of the eutectic solid phase for Sn-8.12 at% Mg-4.97 at% Zn alloy and the thermal conductivity ratio of the liquid phase to the solid phase for Sn-8.12 at% Mg-4.97 at% Zn alloy at eutectic temperature were also measured with a radial heat flow apparatus and a Bridgman-type growth apparatus, respectively. The Gibbs-Thomson coefficient, solid-liquid interfacial energy and grain boundary energy of solid Sn in equilibrium with Sn-Mg-Zn liquid were determined to be (8.3 ± 0.6)×10-8 Km, (118.5 ± 14.2)×10-3 J m-2 and (225.1 ± 29.3)×10-3 J m-2 respectively from observed grain boundary groove shapes. A comparison of present results for solid Sn in the Sn-8.12 at% Mg-4.97 at% Zn alloy with the results obtained in previous works for similar solid Sn in equilibrium with different binary or ternary liquid was made.Article The Experimental Determination of Interfacial Energies for Solid Zn in Equilibrium with Zn-Al-Sb Liquid(SPRINGER, 2015) Altintas, Yemliha; Ozturk, Esra; Aksoz, Sezen; Keslioglu, Kazim; Marasli, Necmettin; AGÜ, Mühendislik Fakültesi, Malzeme Bilimi ve Nanoteknoloji Mühendisliği Bölümü; Altintas, YemlihaThe equilibrated grain boundary groove shapes of solid Zn in equilibrium with Zn-Al-Sb liquid were observed from a quenched sample using a radial heat flow apparatus. The Gibbs-Thomson coefficient, solid-liquid interfacial energy, and grain boundary energy of the solid Zn were determined from the observed grain boundary groove shapes. The thermal conductivity of the eutectic solid phase for Zn-0.4 at. pct Al-0.4 at. pct Sb alloy and the thermal conductivity ratio of the liquid phase to the solid phase for Zn-0.4 at. pct Al-0.4 at. pct Sb alloy at eutectic temperature were also measured with a radial heat flow apparatus and a Bridgman-type growth apparatus, respectively.Article The experimental determination of thermophysical properties of intermetallic CuAl2 phase in equilibrium with (Al plus Cu plus Si) liquid(ACADEMIC PRESS LTD- ELSEVIER SCIENCE LTD24-28 OVAL RD, LONDON NW1 7DX, ENGLAND, 2016) Altintas, Yemliha; Aksoz, Sezen; Keslioglu, Kazim; Marasli, Necmettin; AGÜ, Mühendislik Fakültesi, Malzeme Bilimi ve Nanoteknoloji Mühendisliği Bölümü; Altintas, YemlihaThe equilibrated grain boundary groove shapes of solid CuAl2 in equilibrium with (Al + Cu + Si) eutectic liquid were observed from a quenched sample by using a radial heat flow apparatus. The Gibbs-Thomson coefficient, (solid + liquid) interfacial energy and grain boundary energy of the solid CuAl2 were determined from these observed shapes. The thermal conductivity of the eutectic solid and the thermal conductivity ratio of eutectic liquid to the eutectic solid in the (Al + 26.82 wt.% Cu + 5.27 wt.% Si) eutectic alloy at its eutectic melting temperature were also measured with a radial heat flow apparatus and a Bridgman-type growth apparatus, respectively. The three phases of (Al + Cu + Si) alloy have detected as Al solution, Si and theta (CuAl2) phases with EDX composition analysis and the microstructure of these phases were photographed by SEM. (C) 2016 Elsevier Ltd. All rights reserved.Article Experimental measurements of some thermophysical properties of solid CdSb intermetallic in the Sn-Cd-Sb ternary alloy(SPRINGERVAN GODEWIJCKSTRAAT 30, 3311 GZ DORDRECHT, NETHERLANDS, 2016) Ozturk, Esra; Aksoz, Sezen; Altintas, Yemliha; Keslioglu, Kazum; 0000-0002-1993-2655; AGÜ, Mühendislik Fakültesi, Malzeme Bilimi ve Nanoteknoloji Mühendisliği Bölümü; Altintas, YemlihaThe equilibrated grain boundary groove shapes of solid CdSb in equilibrium with Sn-Cd-Sb eutectic liquid were observed from a quenched sample by using a radial heat flow apparatus. The Gibbs-Thomson coefficient, solid-liquid interfacial energy and grain boundary energy of the solid CdSb intermetallic were determined from the observed grain boundary groove shapes. The thermal conductivity of the eutectic solid and the thermal conductivity ratio of eutectic liquid to the eutectic solid in the Sn-35.8 at.%Cd-6.71 at.%Sb eutectic alloy at its eutectic melting temperature were also measured with a radial heat flow apparatus and a Bridgman-type growth apparatus, respectively.Article The measurements of electrical and thermal conductivity variations with temperature and phonon component of the thermal conductivity in Sn-Cd-Sb, Sn-In-Cu, Sn-Ag-Bi and Sn-Bi-Zn alloys(ELSEVIER FRANCE-EDITIONS SCIENTIFIQUES MEDICALES ELSEVIER65 RUE CAMILLE DESMOULINS, CS50083, 92442 ISSY-LES-MOULINEAUX, FRANCE, 2016) Altintas, Yemliha; Kaygisiz, Yusuf; Ozturk, Esra; Aksoz, Sezen; Keslioglu, Kazim; Marasli, Necmettin; AGÜ, Mühendislik Fakültesi, Malzeme Bilimi ve Nanoteknoloji Mühendisliği Bölümü; Altintas, YemlihaThe electrical and thermal conductivity variations with temperature for lead-free ternary solders, namely Sn-41.39 at.% Cd-6.69 at.% Sb, Sn-49 at.% In-1 at.% Cu, Sn-50 at.% Ag-10 at.% Bi and Sn-32 at.% Bi-3 at.% Zn alloys, were measured by the d.c. four-point probe method and radial heat flow apparatus, respectively. The contributions of electrons and phonons to the thermal conductivity were separately determined by using the measured values of the thermal and electrical conductivities obtained by the Wiedemann-Franz law in the lead-free ternary solders. The percentages of the phonon component of thermal conductivity were found to be in the range of 46-55%, 46-50%, 38-47% and 69-73% for Sn-41.39 at.% Cd-6.69 at.% SU, Sn-49 at.% In-1 at.% Cu, Sn-50 at.% Ag-10 at.% Bi and Sn-32 at.% Bi-3 at.% Zn alloys at the ranges of 318-443 K temperature, respectively. The temperature coefficients (alpha) of electrical conductivity for the lead-free ternary solders were found to be 2.47 x 10(-3), 4.97 x 10(-3), 1.14 x 10(-3) and 1.00 x 10(-3) K-1, respectively. The thermal conductivities of the solid phases at their melting temperature and the thermal temperature coefficients for the lead-free ternary solders were also found to be 47.72 +/- 2.38, 68.57 +/- 3.42, 73.52 +/- 3.67, 37.53 +/- 1.87 W/Km and 1.47 x 10(-3), 1.48 x 10(-3), 1.85 x 10(-3) and 2.21 x 10(-3) K-1, respectively. (C) 2015 Elsevier Masson SAS. All rights reserved.Article Thermal conductivity and interfacial energy of solid Bi in the Bi-Ag eutectic system(SPRINGER, 2015) Altintas, Yemliha; Ozturk, Esra; Aksoz, Sezen; Keslioglu, Kazim; Marasli, Necmettin; AGÜ, Mühendislik Fakültesi, Malzeme Bilimi ve Nanoteknoloji Mühendisliği Bölümü; Altintas, YemlihaThe equilibrated grain boundary groove shapes for solid Bi (Bi–2.87 at.%Ag) in equilibrium with Bi–Ag eutectic liquid have been observed from quenched sample with a radial heat flow apparatus. The Gibbs–Thomson coefficient, solid–liquid interfacial energy and grain boundary energy of solid Bi have been determined from the observed grain boundary groove shapes. The variation of thermal conductivity with temperature for eutectic solid phase (Bi–4.7 at.%Ag) has been measured. The ratio of thermal conductivity of equilibrated eutectic liquid phase to eutectic solid phase has also been measured with a Bridgman-type growth apparatus at the melting temperature. The Gibbs–Thomson coefficient, solid–liquid interfacial energy and grain boundary energy of solid Bi in equilibrium with Bi–Ag eutectic liquid were determined to be (9.2 ± 0.6) 9 10–8 K m, (52.7 ± 6.3) 9 10–3 J m–2 and (102.4 ± 13.3) 9 10–3 J m–2, respectively, from observed grain boundary groove shapes.Article The variations of electrical resistivity and thermal conductivity with growth rate for the Zn-Al-Cu eutectic alloy(SPRINGERVAN GODEWIJCKSTRAAT 30, 3311 GZ DORDRECHT, NETHERLANDS, 2021) Marasli, Necmettin; Bayram, Umit; Aksoz, Sezen; 0000-0001-8760-8024; AGÜ, Yaşam ve Doğa Bilimleri Fakültesi, Biyomühendislik Bölümü; Bayram, UmitThe Zn-Al-Cu alloy (Zn-5wt%Al-0.5wt%Cu) is solidified with different growth rates (V = 8.45-2087.15 mu m s(-1)) at a constant temperature gradient (G = 3.67 K mm(-1)) using Bridgman-type directional solidification apparatus (BTDSA). The thermal conductivity (K) and electrical resistivity (rho) for the Zn-Al-Cu alloy solidified with the different V values are measured by the longitudinal heat flow method (LHFM) and DC four-point probe technique (FPPT), respectively. The lambda and K decrease with the increasing V, while the q increases with increasing V in the Zn-Al-Cu eutectic alloy. The dependences of rho and K on lambda and V for the Zn-Al-Cu eutectic alloy are obtained as rho = 9.98 x 10(-8)lambda(-0.18), q = 7.03 x 10(-8) V-0.07, K = 110.91 lambda(0.104) and K = 144.59V(-0.040), respectively. The melting enthalpy (DHf) and specific heat difference between solid and liquid phases (Delta C-p) for the Zn-Al-Cu eutectic alloy are determined as 113.89 J g(-1) and 0.172 J g(-1) K-1, respectively, by the differential scanning calorimetry (DSC).